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Isothermal microcalorimetry Isothermal titration calorimetry Dynamic mechanical analysis Thermomechanical analysis Thermogravimetric analysis Differential thermal analysis Dielectric thermal analysis. In this mode the sample will be housed in a non-reactive crucible often gold or gold-plated steel , and which will be able to withstand pressure typically up to bar. By observing the difference in heat flow between the sample and reference, differential scanning calorimeters are able to measure the amount of heat absorbed or released during such transitions. It was shown from the obtained results that low heating rates are more suitable for PCMs scanning during DSC measurements in order to ensure a thermodynamic equilibrium within the sample.
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